Low-temperature synthesis of 0.65 PbMg1/3Nb2/3O3-0.35PbTiO(3) ceramics

Sen, S and Das, Swapan K and Mishra, Suman K and Tarafder, A (2007) Low-temperature synthesis of 0.65 PbMg1/3Nb2/3O3-0.35PbTiO(3) ceramics. Journal of the American Ceramic Society, 90 (8). pp. 2634-3638.

Full text not available from this repository.


Nanocrystalline 0.65 PbMg1/3Nb2/3O3-0.35PbTiO(3) powders were synthesized by citrate gel method. The gel was prepared using citrate (titanium and niobium) and nitrate (lead and magnesium) salts. The hard gel obtained after completion of the reaction was treated to get the desired phase. Thermal analysis of the gel was done to optimize the calcination temperature. The calcined powders were characterized by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The crystallite size and the effective strain were found to be 50nm and 0.03584 N, respectively.

Item Type:Article
Official URL/DOI:DOI: 10.1111/j.1551-2916.2007.01757.x
Uncontrolled Keywords:lead magnesium niobate; citrate-gel; system; oxide
Divisions:Material Science and Technology
ID Code:3424
Deposited On:18 Jul 2011 12:41
Last Modified:22 Nov 2011 10:54
Related URLs:

Repository Staff Only: item control page