Single step synthesis of Ni wire, sponge and flower, and their magnetic properties

Sahu, Ranjan K and Roy, Ajoy K and Manotiaran, S S and Arora, S and Mishra, T and Lim, S -H and Salamanca-Riba, L G and Kundaliya, D C and Panda, A K and Mitra, A and Pathak, L C (2008) Single step synthesis of Ni wire, sponge and flower, and their magnetic properties. Magnetic Materials Book Series: Aip Conference Proceedings, 1003 . pp. 100-102.

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Abstract

We reported a single step process for the synthesis of Ni having wire, sponge and flower type microstructures that are obtained via a microwave-assisted decomposition of Ni-TEA (triethanolamine) complex precursor with and without amino acid. The products formed at different stages of the growth process were characterized using scanning electron microscope (SEM), transmission electron microscope (TEM) and magnetometer. Morphological modification enhanced the coercivity from 40 Oe for the Ni-wire to 120 Oe for the Ni-flower with exchange bias effect, which mechanistically arises due to the presence of NiO phase.

Item Type:Article
Official URL/DOI:http://apps.isiknowledge.com/full_record.do?produc...
Uncontrolled Keywords:magnetic nanoparticles; microwave synthesis; magnetic properties
Divisions:Material Science and Technology
ID Code:3305
Deposited By:Sahu A K
Deposited On:13 Jul 2011 12:09
Last Modified:02 Jul 2012 17:49
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