A rapid flame atomic absorption spectroscopic procedure for determination of lead in aluminium base alloys

Rao, Addanki S and Gupta, K K and Sircar, J K and Srivastava, S C (2004) A rapid flame atomic absorption spectroscopic procedure for determination of lead in aluminium base alloys. Indian Journal Of Chemical Technology , 11 (4). pp. 475-478.

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Abstract

A rapid and sensitive technique to determine lead in trace level present in aluminium based alloys by flame atomic absorption spectroscopic technique (AAS) is described. It is free from aluminium and silicon spectral interferences. The method is free from associated alloying elements. Lead was determined at 283.3 nm using air-acetylene flame. The value of relative standard deviation (r.s.d.) of lead, in case of high silicon containing samples is found to be 2.545% and that for low ones 10-12% respectively. The standard deviation values were +/-0.0014 and +/-0.0016 respectively. A threshold limit of concentration of aluminium and silicon for the determination of lead in final analyte solution has been described and this has been correlated with the sample weight to be taken for analysis.

Item Type:Article
Official URL/DOI:http://apps.webofknowledge.com/full_record.do?prod...
Uncontrolled Keywords: lead determination; alluminium alloy; atomic absorption spectroscopy
Divisions:Analytical Chemistry
ID Code:3625
Deposited By:Sahu A K
Deposited On:27 Jul 2011 12:51
Last Modified:08 Feb 2012 14:14
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